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Microwave-Assisted Synthesis Of Alkyl Thiocyanates.
James Bound, D. and Bettadaiah, B. K. and Srinivas, P. (2013) Microwave-Assisted Synthesis Of Alkyl Thiocyanates. Synthetic Communications, 43. pp. 1138-1144.
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Synthetic CommunicationsVolume 43, Issue 8, April 2013, pages 1138-1144.pdf - Published Version Restricted to Registered users only Download (241kB) |
Abstract
Microwave irradiation accelerated the reaction of t-alkyl, allyl, and benzyl halides with Zn(SCN)2 to afford thiocyanates in excellent yields and high selectivity with the formation of isothiocyanates only in minor proportions. Because thiocyanates are stable intermediates to thiols, the method also affords facile access to corresponding thiols.
| Item Type: | Article |
|---|---|
| Uncontrolled Keywords: | Allyl; benzyl; halides; isothiocyanates; microwave; selectivity; t-alkyl; thiocyanates; zinc thiocyanate |
| Subjects: | 600 Technology > 08 Food technology > 15 Flavour/Fragrance/Perfumes 600 Technology > 08 Food technology > 06 Preservation and Storage > 04 Irradiation |
| Divisions: | Plantation Products Spices and Flavour Technology |
| Depositing User: | Food Sci. & Technol. Information Services |
| Date Deposited: | 26 Apr 2013 09:08 |
| Last Modified: | 12 Jun 2019 08:46 |
| URI: | http://ir.cftri.res.in/id/eprint/11202 |
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